1. Analysis:
Segments are made of Cu xx %, Fe yy % and Co zz %. This is conform to the analysis you gave us.
2. Metallography:
On the SEM picture enclosed, you will clearly observe that the addition of carbonyl iron has not diffused in the matrix. This is most probably due to a low sintering temperature.
The carbonyl iron is spherical and we can clearly see the border of the grains (see the dark grey spots on the picture).
On the contrary, the probability exists that carbonyl iron particles were subject to high oxidization.
Conclusion: the addition of carbonyl iron was not necessary.
3. Working Surface:
One can clearly see on the SEM pictures that the working surface of the segments looks normal. The number of “pulls-out” looks normal too.
But, we can clearly observe that the diamonds have a strong tendance to polish. This mainly explains why the discs stopped cutting after a while.
4. Diamonds:
5 segments were disolved into acid baths and diamonds have been submitted to an extra-cleaning.
The concentration is about C19. The size of the diamonds is clearly a 50/60 Mesh. Diamonds 60/70 Mesh are not found.